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CRE 02
ISOTHERMAL CONTINUOUSLY STIRRED TANK REACTOR (ISOTHERMAL CSTR)
DESCRIPTION
In an ideal CSTR (Le. an ideal steady state flow reactor) the contents in reactor are well mixed and have uniform composition throughout. Thus the exit stream has the same composition as the fluid within the reactor. This type of reactor is known as mixed flow reactor. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under isothermal condition. The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. The CSTR is fitted with stirrer for proper mixing. From top outlet of it samples are collected for analysis. Constant temperature water bath arrangement is provided to conduct the experiment at various temperatures. Pressure Regulator, Pressure Gauge and Safety Valves are fitted in the compressed air line
EXPERIMENTS
- Saponification Reaction study in Isothermal CSTR
- To determine the Reaction Rate Constant and effect of temperature on it
UTILITIES REQUIRED
- Compressed Air Supply at 2 Bar, 0.5CFM.
- Water Supply & Drain
- Electricity Supply: 1 Phase, 220VAC, 1.5kW.
- Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted
Product & Code |
Isothermal Continuously Stirred Tank Reactor (CSTR) & CRE 02 |
Reactor |
Material Stainless Steel, Capacity 2 Ltrs. (Approx) |
Water Bath |
Material Stainless Steel, Double wall, insulated with Ceramic Wool |
Heater |
Nichrome wire Heater |
Stirrer(2Nos.) |
Stainless Steel Impeller and shaft coupled with FHP motor. (One each for Water Bath and Reactor) |
Feed Tank(2Nos.) |
Material Stainless Steel (2 Nos.), Capacity 20 Ltrs. with level indicators, air release valves, charging funnel with valve, air pressure fittings, feed lines, drain valve etc. |
Feed Circulation |
By Compressed Air, using PU pipe line & fittings Pressure Regulator Bourdon type (0-2 kg/cm2) |
Flow Measurement |
Rotameter 2Nos. (one each for Reactants) |
Feed Piping |
PVC / SS |
Stop Watch |
Electronic |
Temp. Sensor |
RTD PT-100 type |
Control panel |
Digital Temp. Controller: 0- J.99.9°C (For Hot Water Bath), On/off switch, Mains Indicator etc. |
The setup is painted with good quality paints & mounted on a strong support. |
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