CRE 06 ISOTHERMAL PLUG FLOW TUBULAR REACTOR (COILED TUBE TYPE)

DESCRIPTION

 

In an ideal Plug Flow Reactor {PFTP} there is no mixing in the direction of flow and complete mixing perpendicular to direction of flow. Concentration of reactants varies along the length of reactor but not in radial direction. In case of a coil turbulence is introduced due to frequent change in direction of flow and presence of secondary flow, so a higher value of reaction rate constant is expected in coil tube type plug flow reactor. This set- up is used to study a non-catalytic homogeneous reaction under isothermal condition. The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. It is a helical coil tube type reactor kept in a constant temperature water bath to conduct the experiment at various temperatures. Reactants enter at lower end coming out of the top of coil from where samples are collected for analysis. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line

EXPERIMENTS

 

  • Saponification Reaction study in Isothermal Plug flow Reactor
  • To determine Reaction Rate Constant and effect of temperature on it

 

UTILITIES REQUIRED

 

  • Compressed Air Supply at 2 Bar, 0.5 CFM
  • Water supply and drain
  • Electricity-1.5kw, Single
  • Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted

TECHNICAL DETAILS

Product & Code Isothermal Plug Flow Tubular Reactor (Coiled Tube Type) & CRE 06
Reactor Material Stainless Steel, Capacity 0.7 Ltrs. (approx) (Helical Coiled Tube Type)
Water Bath Material Stainless Steel, Double wall, insulated with Ceramic Wool.
Heater Nichrome wire Heater
Stirrer(for Water Bath) Stainless Steel Impeller and shaft coupled with FHP motor.
Feed Tank (2Nos.) Material Stainless Steel (2 Nos.), Capacity 20 Ltrs. with level indicators, air release valves, charging funnel with valve, air pressure fittings, feed lines, drain valve etc.
Feed Circulation By Compressed Air, using PU pipe line & fittings Pressure Regulator Bourdon type (0-2 kg/cm2)
Flow Measurement Rotameter 2Nos. (one each for Reactants)
Feed Piping PVC / SS
Stop Watch Electronic
Temp. Sensor RTD PT-100 type
Control panel  Digital Temp. Controller: 0-200°C. RTD PT-100type (For Water Bath) On/off switch, Mains Indicator etc.
The setup is painted with good quality paints & mounted on a strong support.
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