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CRE 15
EMULSION POLYMERIZATION REACTOR
DESCRIPTION
The set-up consists of jacketed type SS reactor fitted with a variable speed agitator & baffles. Hot water from a digitally controlled water bath is circulated in the jacket using a pump. Metered quantity of nitrogen gas from a cylinder passes through a de -oxygenation column & allowed to enter in the reactor. Air has to be evacuated using a vacuum pump to create vacuum up to 30mm of Hg before passing the nitrogen supply. Initiator from reservoir is supplied to the reactor under pressure. Set-up is complete& self-contained with sampling ports
EXPERIMENTS
- Effect of monomer concentration
- Effect of Initiator concentration.
- Effect of emulsifier concentration.
- Effect of RPM on conversion.
UTILITIES REQUIRED
- Water supply and drain.
- Electricity- 1.5kw, Single.
- Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.
- Vacuum Pump
- High purityN2 gas
| Product & Code |
Emulsion Polymerization Reactor & CRE 15 |
| Reactor (Jacketed Type) |
Material Stainless Steel Total volume of Reactor 1.5 /2 Ltrs. (approx.) |
| Agitator |
Material Stainless Steel Impeller (2 paddles) fitted with Stainless Steel Shaft coupled to Motor with control Drive. |
| Flow Measurement |
Rotameter for Nitrogen Gas. |
| De-Oxygenation Column |
Compatible capacity. |
| Hot Water Tank |
Material Stainless Steel, Double Wall, insulated with ceramic wool. |
| Hot water circulation |
Magnetic Pump made of Polypropylene. Maximum working temperature is 80°C. |
| Heaters |
Nichrome wire heater. |
| Initiator Reservoir |
Capacity 25-50ml. |
| Control panel |
On/off switch, Mains Indicator etc. Digital Temp. Indicator 0-199.9°C, RTD PT-100type (with Multi-channel switch) Digital Temp Controller 0-I99.9°C RTD PT-100type (For hot water tank) RPM Indicator Digital, Non-contact type |
| Temp. Sensors |
RTD PT-I00type (5 Nos) |
| Vacuum Pump |
Compatible capacity is provided |
| N2 Cylinder |
N2 Cylinder with regulator is provided |
| The setup is painted with good quality paints & mounted on a strong support. |
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