CRE 19 RECYCLE BED REACTOR

DESCRIPTION

 

The setup consist a catalyst packed column of Stainless Steel. Reactant from a fed tank is fed to the reactor through liquid distributor, fitted at one end of the column. Some part of product is recycled to the reactor using a low capacity sophisticated pump or by over head tank system. Rotameters are provided to measure the flow of feed & recycled product. The feed rate and recycle product ratio can be manipulated by the respective needle valves of the rotameter. Samples can be taken periodically from the top outlet of reactor at another end. An arrangement is made to carry out the reaction at Isothermal conditions by circulating the hot water in the outer jacket of the packed bed reactor. Special care is taken for proper mixing of feed & recycle product before its entry to the reactor. A magnetic drive pump made up of polypropylene is used for circulation of feed.

EXPERIMENTS

 

  • To determine the Reaction Rate Constant.

 

UTILITIES REQUIRED

 

  • Water Supply & Drain
  • Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted

TECHNICAL DETAILS

Product & Code Recycle Bed Reactor & CRE 19
Reactor Column Material Stainless Steel Diameter 1″ or 1 ½”, Length: 750mm.
Packing Catalyst
Feed Tank ( I Nos.) Material Stainless Steel, Capacity -20 Ltrs
Flow Measurement Rotameter 2 Nos (One each for feed & recycled product)
Piping Stainless Steel and PVC. Size ¼ “
Feed Circulation Magnetic Pump of Poly propylene
Hot water tank Mace of Stainless steel, Double wall, insulated with Ceramic Wool. Capacity: 10-15 Ltrs
Hot water Circulation

(in outer Jacket):

Magnetic Pump of Poly propylene to circulate Hot Water maximum working temp. 80 0 C
Heaters Nichrome wire heater 750-1000 W approx.
Control panel On/Off switch, Mains Indicator & fuse etc., Digital Temperature Controller 0-200°C RTD, PT-I00 type (For Hot Water Tank)
The setup is painted with good quality paints & mounted on a strong support.
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