CRE 20 SPINNING BASKET REACTOR

DESCRIPTION

 

Any catalytic liquid-liquid or liquid-gas reaction involving the use of a catalyst placed in basket can be studies in this set-up. Kinetic parameter of a specific reaction can be estimated & parametric studies can be conducted. The set-up consists of a reactor centrally having one spinning basket derived through a variable speed motor. The metered flow of reactant from feed tank is fed to the reactor at the bottom. The set-up can be used as batch wise of as continuous type. Sampling points are provided for analysis. Port connection for gas inlet is provided at the bottom of the reactor.

EXPERIMENTS

 

  • To determine the kinetic parameters for a given reaction

 

UTILITIES REQUIRED

 

  • Compressed air supply at 1Bar
  • Water Supply& Drain
  • Power Supply: 0.5 kW, Single Phase.
  • Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted

TECHNICAL DETAILS

Product & Code Spinning Basket Reactor & CRE 20
Reactor Vessel Material SS Effective Volume: 1000 ml.
Basket Material Stainless Steel, Fitted with appropriate Stainless Steel.
Drive for Basket DC Motor with Thyristor controlled DC Drive for Variable Speed.
Packing Catalyst
Feed Tank (l Nos.) Material Stainless Steel, Capacity – 10 Ltrs.
Flow Measurement Rotameter,
Pressure regulator Operating Range 0-2 kg/cm2
Pressure Gauge Bourdon Type 0-2 kg/cm2
Receiver Material Stainless Steel, Capacity 10 Ltrs.
Piping Stainless Steel and PVC. Size 1,4″
Hot water Circulation (in outer Jacket) Magnetic Pump of Poly propylene to circulate Hot Water maximum working temp. 80 0 C
Hot water tank Made of Stainless Steel, Double wall, insulated with Ceramic Wool. Capacity: 10-15 Ltrs.
Heaters Nichrome wire heater 750-1000 W approx.
Temperature Sensors RTD PT-100 Type.
Control panel Digital Temperature Controller 0-200°C RTD PT-100 type (For Hot Water Tank) Digital Temperature Indicator – 0-200°C with multi-channel switch. RPM Indicator – Digital, Non-Contact Type. On/Off switch. Mains Indicator & fuse etc
The setup is painted with good quality paints & mounted on a strong support.
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