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CRE 20
SPINNING BASKET REACTOR
Any catalytic liquid-liquid or liquid-gas reaction involving the use of a catalyst placed in basket can be studies in this set-up. Kinetic parameter of a specific reaction can be estimated & parametric studies can be conducted. The set-up consists of a reactor centrally having one spinning basket derived through a variable speed motor. The metered flow of reactant from feed tank is fed to the reactor at the bottom. The set-up can be used as batch wise of as continuous type. Sampling points are provided for analysis. Port connection for gas inlet is provided at the bottom of the reactor.
EXPERIMENTS
- To determine the kinetic parameters for a given reaction
UTILITIES REQUIRED
- Compressed air supply at 1Bar
- Water Supply& Drain
- Power Supply: 0.5 kW, Single Phase.
- Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted
Product & Code |
Spinning Basket Reactor & CRE 20 |
Reactor Vessel |
Material SS Effective Volume: 1000 ml. |
Basket |
Material Stainless Steel, Fitted with appropriate Stainless Steel. |
Drive for Basket |
DC Motor with Thyristor controlled DC Drive for Variable Speed. |
Packing |
Catalyst |
Feed Tank (l Nos.) |
Material Stainless Steel, Capacity – 10 Ltrs. |
Flow Measurement |
Rotameter, |
Pressure regulator |
Operating Range 0-2 kg/cm2 |
Pressure Gauge |
Bourdon Type 0-2 kg/cm2 |
Receiver |
Material Stainless Steel, Capacity 10 Ltrs. |
Piping |
Stainless Steel and PVC. Size 1,4″ |
Hot water Circulation (in outer Jacket) |
Magnetic Pump of Poly propylene to circulate Hot Water maximum working temp. 80 0 C |
Hot water tank |
Made of Stainless Steel, Double wall, insulated with Ceramic Wool. Capacity: 10-15 Ltrs. |
Heaters |
Nichrome wire heater 750-1000 W approx. |
Temperature Sensors |
RTD PT-100 Type. |
Control panel |
Digital Temperature Controller 0-200°C RTD PT-100 type (For Hot Water Tank) Digital Temperature Indicator – 0-200°C with multi-channel switch. RPM Indicator – Digital, Non-Contact Type. On/Off switch. Mains Indicator & fuse etc |
The setup is painted with good quality paints & mounted on a strong support. |
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