The unit consists of a packed column with borosilicate ranching rings or ceramic berl saddles. A glass flask with a heating mantle is used as a reactor vessel. The condenser is provided with copper/glass coil in which cooling water is circulated. The flow rate of cooling water is measured by the Rotameter and the temperatures of various systems are also measured. A stirrer assembly with FHP flame proof motor a mechanical stirrer and a agitator with speed regulator is also provided.
The density of bottom and reflux can be measured by using specific gravity or by the method of refractive index
UTILITIES REQUIRED
Water Supply & Drain
Electricity Supply: 1Phase, 220 V AC, 1.5 kW
Refractrometer for Analysis
Vacuum pump ¼ HP 2 stage oil seal type with moisture trap
Required Chemicals
TECHNICAL DETAILS
Product & Code
Fractional Reaction Distillation Unit and MT 29
Reactor Vessel
Glass Flask Capacity: 5 Ltr, material borosilicate glass
Heating Mantle
Suitable capacity for 5 ltr flask
Stirrer Unit
Flame proof FHP motor with glass / Teflon stirrer, mechanical seal, speed regulator etc.
Packed column
Size dia 1”, height 750 mm approx
Packing material
Rasching Ring 8-10 mm Material Borosilicate Glass
Condenser
Concentric Tube type Material borosilicate glass
Cooling Water Tank
Material Stainless Steel, Capacity 20 Ltrs
Cold Water circulation
Using FHP Pump.
Flow measurement
Cooling water flow measurement by using rotameter
Receiver
1000 ml, 500 ml (1 no each)
Temperature Sensors
RTD PT-100 type
Control panel
Temperature Controller for heating mantle, RTD PT 100 type (199.9°C, 0.1°C least count)
Digital temperature indicator:0-199.90C RTD PT-100 Type with multi-channel switch, On/off switch, Mains Indicator etc
