MT 30 FRACTIONAL DISTILLATION (DISTILLATION AT TOTAL REFLUX)

Description

 

The unit consists of a packed column with borosilicate ranching rings or ceramic berl saddles. Four necked glass flask with a heating mantle is used as a re boiler.  This system is designed for methanol-water mixture.  The condenser is provided with copper/glass coil in which cooling water is circulated.  The flow rate of cooling water is measured by the Rotameter and the temperatures of various systems are also measured. The density of bottom and reflux can be measured by using specific gravity or by the method of refractive index

 

UTILITIES REQUIRED

 

  • Water Supply & Drain
  • Electricity Supply: 1Phase, 220 V AC, 1.5 kW
  • Refractrometer for Analysis
  • Vacuum pump ¼ HP 2 stage oil seal type with moisture trap
  • Required Chemicals

 

TECHNICAL DETAILS

                                                            

Product & Code Fractional Distillation & MT-30
Re boiler Glass Flask Capacity: 5 Ltr, four necked flask material borosilicate glass
Packed column Size dia 1”, height 750 mm approx ,
Packing material Rasching Ring 8-10 mm Material Borosilicate Glass
Condenser Concentric Tube type Material of construction borosilicate glass
Flow measurement Cooling water flow measurement by using rotameter
Receiver 1000 ml, 500 ml (1 no each)
Heating Mantle Suitable capacity for 5 ltr flask
Cooling Water Tank Material Stainless Steel, Capacity 20 Ltrs
Cold Water circulation Using FHP Pump.
Temperature Sensors RTD PT-100 type
Control panel Temperature Controller for heating mantle PID Controller, RTD PT 100 type (199.9°C, 0.1°C least count)Digital temperature indicator:0-199.90C RTD PT-100 Type with multi-channel switch On/off switch, Mains Indicator etc
Major accessory components Drain valve, Thermometer/RTD sensor pocket, reflux divider, vent valve, product cooler, intermediate receiver, vacuum stop and release valve and receiver flask
The whole set-up is fixed on a structure.
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